Chemistry 3150: Advanced Inorganic Laboratory

Fall 2007, Laney 305, Tu: 2:40 – 5:40 pm   

Text Box: Fall 2007 Syllabus Text Box: Lab writeup advice Text Box: Useful References
 

 

 

 

 


Experiments

Text Box: UV-vis

Text Box: IR

Text Box: NMR

Text Box: EPR

Text Box: Magnetic Susceptibility

Text Box: E-Chem

Other

First Day Practice

X

X

 

X

 

 

inert atmosphere cannula transfer

HxWO3

H2 intercalation

 

 

X

 

 

X

 

        conductivity

doped ZnS

phosphors

 

 

 

 

 

 

 

UV exposure

fluorescence?

Tube furnace

Cu(Gly-Gly)

hydroxyl radicals

 

X

 

 

X

 

 

 

Co-catalyzed

tartrate oxidation

 

X

 

 

 

 

 

 

Metal Complex

UVvis/magnetism

 

X

 

59Co?

 

X

 

 

Co-NO2

linkage isomers

 

X

Temperature

dependent

59Co?

 

 

 

 

Metal-Metal

multiple bonds

 

X

X

1H, 13C

 

 

 

inert

atmosphere

RuCl2(dppb)(phen)

isomerism

 

 

 

31P

 

 

X

inert

atmosphere

M porphyrins

 

X

 

X

 

X

 

 

 

References on 2 hour reserve
mNakamoto, K. Infrared Spectra of Inorganic and Coordination Compounds (2nd); Wiley Interscience: N.Y., 1970.
mCotton, F. A.; Wilkinson, G. Advanced Inorganic Chemistry (4th); Wiley Interscience: New York, 1980.
mGreenwood, N. N.; Earnshaw, A. Chemistry of the Elements; Pergammon Press: New York, 1984.
mDrago, R. S. Physical Methods in Chemistry W. B. Saunders Co.: Philadelphia, 1977.
mJolly, W. L. Synthesis and Characterization of Inorganic Compounds Waveland Press: Prospect Heights, IL,       1991.
mHammond, C. The Basics of Crystallography and Diffraction American Chemical Society, 1998

General reference: some I have, some the library has
mInorganic Syntheses Wiley, New York.  Torreyson Library has volumes 1-32(1998).
lEllis, A. B.; Geselbracht, M. J.; Johnson, B. J.; Lisensky, G. C.; Robinson, W. R.  Teaching General Chemistry, A Materials Science Companion American Chemical Society: Wash. D.C., 1993.
lPough, F. H. A Field Guide to Rocks and Minerals (4th) Houghton Mifflin Co.: Boston, 1976.

Other useful references (recent general chemistry textbooks)
mMoore, J. W.; Stanitski, C. L.; Wood, J. L.; Kotz, J. C. The Chemical World Saunders College Publishing: Ft. Worth, TX, 1998.
mKotz, J. C.; Purcell, K. F. Chemistry & Chemical Reactivity (2nd); Saunders College Publishing: Ft. Worth, TX, 1991,  pp. 438-42, 1025-66.
mKotz, J. C.; Joesten, M. D.; Wood, J. L.; Moore, J. W. The Chemical World: Concepts and Applications; Saunders College Publishing: Ft. Worth, TX, 1994, pp. 441-6, 490-8, 619-39.